The Rites of Hajj (Kitab Al-Manasik Wa'l-Hajj)
Dawud :: Book 10 : Hadith 1891
Narrated Aisha, Ummul Mu'minin:
The Companions of the Apostle of Allah (peace_be_upon_him) who accompanied him did not go round the Ka'bah till they threw pebbles at the Jamrah (pillar at Mina).